测定土壤全钾的几种熔样方法的比较
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COMPARISON OF SEVERAL FUSION METHODS FOR DETERMINATION OF TOTAL POTASSION IN SOILS
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    摘要:

    本文通过四个实验室间协作,对Na2CO3,熔融法、HF消解法、NaOH熔融法测定土壤全钾作了比较实验,结果表明:NaOH法对土壤全钾的测出率平均为Na2CO3法的98.5%,为HF法的99.5%;HF法为Na2CO3法的99.1%.三种方法重复测定的标准差多数未超过0.05(K%),变异系数末超过2%.对标准样品的测定值与标准值比较,绝大多数未超过一个标准差值.NaOH法和HF法对土壤全钾的测定值t检验差异不显著.协作实验表明,两方法的精密度基本等效.因此,在大批量样品的常规分折中,NaOH法可代替HF法.

    Abstract:

    This paper deals with a comparative and collaborative study on determining soil total potassium with three fusion or digestion methods conducted by four labortories.The result showed that the average percentage of soil total K value by NaOH fusion method was 98.5% of the value by Na2CO3 fusion method,and 99.5% of the value by HF digestion method.The precision and accuracy of the three methods were also very close.Therefore,the authors sugBest that the NaOH fusion method can be used in routine work instead of HF digestion meshod for determining soil total potassium.

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傅绍清,王永真,张汝英,赵明德.测定土壤全钾的几种熔样方法的比较[J].土壤学报,1989,26(4):324-330. Fu Shaoqing, Wang Yongzhen, Zhang Ruying, Zhao Deming. COMPARISON OF SEVERAL FUSION METHODS FOR DETERMINATION OF TOTAL POTASSION IN SOILS[J]. Acta Pedologica Sinica,1989,26(4):324-330.

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  • 在线发布日期: 2013-02-25
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