激光衍射法和吸管法测定东北黑土区土壤机械组成的比较研究
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东北师范大学

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国家自然科学基金项目(42477345,41401304)和国家重点基础研究发展计划项目(2018YFC0507005)资助


Comparison of Soil Particle Size Distribution in the Black Soil Region of Northeast China Measured by Laser Diffraction Method and the Sieve-Pipette Method
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Northeast Normal University

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Supported by the National Natural Science Foundation of China (Nos. 42477345, 41401304) and National Key Basic Research and Development Program Project (No. 2018YFC0507005)

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    摘要:

    激光衍射法(简称“激光法”)因具备操作简便、测定效率高等优势,近年来在土壤机械组成测定中得到广泛应用。然而,受测定原理和实验流程尚未统一等因素影响,激光法所得土壤机械组成与传统吸管法之间的可比性仍然不足。本研究旨在比较激光法与吸管法测定东北黑土区土壤机械组成的差异特征,并分别基于回归分析法和林氏一致性相关系数法构建激光法向吸管法体系转换的校正模型。为此,采集了该地区36个主要土种的土样,分别采用激光法和吸管法开展土壤机械组成测定。结果表明:(1)两种方法所得土壤机械组成存在显著差异。相较于吸管法,激光法低估了所有土样的黏粒含量,高估所有土样的粉粒含量,而对砂粒含量的差异因样品而异。黏粒、粉粒和砂粒含量的平均绝对差异分别为-30.1%、34.5%和-4.4%。(2)回归分析法校正后,激光法的黏粒、粉粒和砂粒含量的平均绝对差异分别降低至0.9%、0.5%和-1.4%。采用林氏一致性相关系数法优化粒径分级阈值后,黏粒、粉粒和砂粒含量的平均绝对差异降低至1.3%、-3.4%和2.1%。两种方法均显著提高了激光法与吸管法结果的一致性,但回归分析法在计算过程上更为简便。(3)激光法直接判定土壤质地类型的准确率仅为5.6%,表明其原始结果不宜直接用于判定土壤质地分类。经校正后,判定准确率可提升至35%以上。

    Abstract:

    【Objective】The Laser Diffraction Method(LDM) has been increasingly adopted for determining Soil Particle Size Distribution(PSD) due to its rapid measurement speed, high degree of automation, and minimal labor requirement. These advantages make LDM particularly attractive for large-scale soil surveys, laboratory routine analysis, and studies requiring high-resolution particle-size information. Nevertheless, substantial discrepancies persist between PSD measured by LDM and that obtained from the traditional Sieve-Pipette Method(SPM), which remains the reference method in most national and international soil texture classification systems. These inconsistencies arise mainly from differences in measurement principles, contrasting assumptions regarding particle shape and density, the optical models used in LDM instruments, and the absence of unified sample pretreatment protocols. As a result, the direct use of LDM-derived PSD for soil texture classification often yields biased or inconsistent outcomes. Therefore, this study aims to: 1) comprehensively compare PSD measured by LDM and SPM for major soil types in the Black Soil Region(BSR) of Northeast China; and 2) develop and evaluate calibration models based on regression analysis and Lin’s Concordance Correlation Coefficient(CCC) to convert LDM results into an SPM-compatible reference framework. 【Method】Soil samples representing 36 dominant soil series across the BSR, including black soil, chernozem, chestnut Soil, and aeolian Sandy Soil, were collected in the field. After air-drying, the samples were gently ground using a mortar and passed through a 2 mm sieve. PSD for each sample was determined using both LDM and SPM following their respective protocols. Differences in clay, silt, and sand fractions were quantified to characterize systematic deviations. Two calibration strategies were developed: one based on regression analysis, which establishes quantitative relationships between LDM and SPM values using linear regression models; and the other based on Lin’s CCC, which adjusts particle-size cutoff thresholds in LDM to maximize consistency with SPM and identify optimized boundary values for clay, silt, and sand. Model performance was evaluated based on reductions in mean absolute differences and improvements in soil texture classification accuracy using the USDA textural classification system. 【Result】1) Pronounced discrepancies were observed between LDM and SPM. Relative to SPM, LDM consistently underestimated clay content and substantially overestimated silt content across all soil types, whereas deviations in sand content varied depending on sample-specific characteristics. The mean absolute differences for clay, silt, and sand were -30.1%, 34.5%, and -4.4% respectively. 2) Following regression-based correction, the mean absolute differences decreased to 0.9%, 0.5%, and -1.4%, and the accuracy of soil texture classification improved markedly to 36.1%. 3) Lin’s CCC-based calibration further reduced the mean absolute differences to 1.3%, -3.4%, and 2.1%, yielding a classification accuracy of 38.9%. Although both calibration approaches substantially improved agreement between LDM and SPM, the regression-based method was more computationally efficient to apply in routine laboratory workflows. 【Conclusion】Uncorrected LDM-derived PSD is unsuitable for direct soil texture classification in the BSR. However, applying appropriate calibration models, whether regression-based or Lin’s CCC-based, effectively harmonizes LDM data with SPM reference values, significantly enhancing its reliability and practical utility. These findings offer a methodological foundation for integrating LDM into soil survey, monitoring, and classification programs, and provide valuable guidance for improving the comparability of PSD data obtained using different analytical techniques.

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冷子禾,张天宇.激光衍射法和吸管法测定东北黑土区土壤机械组成的比较研究[J].土壤学报,DOI:10.11766/trxb202509270475,[待发表]
LENG Zihe, ZHAGN Tianyu. Comparison of Soil Particle Size Distribution in the Black Soil Region of Northeast China Measured by Laser Diffraction Method and the Sieve-Pipette Method[J]. Acta Pedologica Sinica, DOI:10.11766/trxb202509270475,[In Press]

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  • 收稿日期:2025-09-27
  • 最后修改日期:2026-08-02
  • 录用日期:2026-09-08
  • 在线发布日期: 2026-09-09
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